Showing posts with label Drying of Organic Solvents THF. Show all posts
Showing posts with label Drying of Organic Solvents THF. Show all posts

Drying of Organic Solvents THF, Toluene, MDC (DCM), Acetonitrile, Ether

A recent paper that describes an easier way of drying the common organic solvents than the hazardous, distillation stills.

Reported Procedure :

Analytical reagent- or HPLC-grade solvents were obtained  from commercial sources and used as is or were dried using the  various methods described herein. Desiccants (3 A ° molecular sieves, various silicas, neutral alumina) were obtained from commercial suppliers and were predried at 300 C for 24 h immediately before use. Solvents were dried either by allowing them to stand over the desiccant under nitrogen or by passing the solvent over a column of the desiccant as specified, inside the glove box.. 




Reference : Drying of Organic Solvents : Quantitative Evaluation of the Efficiency of Several Dessicants-
William , G. B. D.; Lawton , M. J. Org. Chem. 2010, ASAP.